20327-23-5, 1-Cyclopropylpiperazine is a piperazines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
20327-23-5, In 100 mL round bottom flask, 1.84 g (10 mmol) of compound II was added, 1.26 g (10 mmol) of compound III-2 and 20 mL of dry THF were added and the resulting mixture was stirred under ice-cooling in water. After adding 2.48 g (12 mmol) of DCC, stirring was continued at room temperature overnight. TLC shows the completion of the reaction.The reaction mixture was poured into ice water, stirred, extracted with 50 mL of X3 in dichloromethane, the combined organic phases were combined, washed with saturated brine, dried over anhydrous sodium sulfate, and the solvent was evaporated on a rotary evaporator. The resulting residue was subjected to column chromatography purification, To give product 1-2 as a white solid.
The synthetic route of 20327-23-5 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Zhejiang Pharmaceutical College; GUO, ZHANG HUA; (6 pag.)CN104356060; (2016); B;,
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