112257-12-2, tert-Butyl 4-(2-bromoacetyl)piperazine-1-carboxylate is a piperazines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Compound D_1 (477 mg, 3 mmol), compound G_1 (1 ¡¤ 38 g, 4.5 mmol), 15 mL of acetonitrile was added to a 50 mL single-mouth flask, and the mixture was heated under argon atmosphere. The mixture was heated under reflux, followed by TLC. Acetonitrile, the residue was dissolved with as little CH2CI2 as possible. A large amount of ether was added to precipitate a solid. The solid was carefully sucked out into an Erlenmeyer flask. It was necessary to allow ether to remain on the surface. The ether was immediately blown dry with argon, and the cone was dried. The bottle is sealed with a sealing membrane and kept out of the air. The product was a pink solid 700 mg (compound H-1) with a yield of 50%., 112257-12-2
112257-12-2 tert-Butyl 4-(2-bromoacetyl)piperazine-1-carboxylate 15829155, apiperazines compound, is more and more widely used in various fields.
Reference£º
Patent; East China University of Science and Technology; Qian Xuhong; Xu Yufang; Jia Xiaotong; Zhu Weiping; Yang Youjun; (14 pag.)CN107619397; (2018); A;,
Piperazine – Wikipedia
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