The effect of the change of synthetic route on the product 18583-60-3

The article 《Di-μ-azido-bis{[hydrotris(pyrazol-1-yl)borato]copper(II)}》 also mentions many details about this compound(18583-60-3)Application In Synthesis of Potassiumtris(1-pyrazolyl)borohydride, you can pay attention to it, because details determine success or failure

Heterocyclic compounds can be divided into two categories: alicyclic heterocycles and aromatic heterocycles. Compounds whose heterocycles in the molecular skeleton cannot reflect aromaticity are called alicyclic heterocyclic compounds. Compound: 18583-60-3, is researched, Molecular C9H10BKN6, about Di-μ-azido-bis{[hydrotris(pyrazol-1-yl)borato]copper(II)}, the main research direction is copper azido pyrazolylborato preparation crystal structure; mol structure copper azido pyrazolylborato.Application In Synthesis of Potassiumtris(1-pyrazolyl)borohydride.

Crystals of the title compound are monoclinic, space group P21/n, with a 7.515(1), b 13.363(2), c 13.285(2) Å, β 93.65(1)°; Z = 2, dc = 1.590; R = 0.049, Rw(F2) = 0.110 for 2605 reflections. The mol. is located at a crystallog. inversion center. The two Cu atoms have distorted square-pyramidal coordination and are bridged by two end-on azide groups. Weak C-H···N contacts result in a two-dimensional network with base vectors [101] and [010], parallel to the (101̅) plane.

The article 《Di-μ-azido-bis{[hydrotris(pyrazol-1-yl)borato]copper(II)}》 also mentions many details about this compound(18583-60-3)Application In Synthesis of Potassiumtris(1-pyrazolyl)borohydride, you can pay attention to it, because details determine success or failure

Reference:
Piperazine – Wikipedia,
Piperazines – an overview | ScienceDirect Topics